The determination of DES and other anabolica in urine and faeces by LC-EC and by HPTLC

T.B.D. van der Struijs, H. Hooijerink, J.M. Weseman, G.M. Binnendijk, A.G. van Leeuwen, D.J. Vonk, W.G. de Ruig

Research output: Book/ReportReportProfessional

Abstract

Methods have been developed for the determination of DES and other anabolica. The sample pretreatment before detection is of great importance. The following methods are described: - DES in a small amount of urine (up to about 5 ml), detection by LC-EC: scheme 1. - DES in a small amount of faeces , detection by LC-EC: scheme 2. - DES in a large amount of urine (25-250 ml), using a specially shaped HPLC pre-column, detection by LC-EC: scheme 3. - Hexestrol, DES and dienestrol in urine, column pretreatment, detection by either HPLTC or LC-EC scheme 4, outline of method on page 14, Results: hexestrol by LC-EC page 16 DES by LC-EC page 17, dienestrol by LC-EC page 18, HPTLC results page 19, densitometry of HPTLC plates: page 20.
Original languageEnglish
Place of PublicationWageningen
PublisherRIKILT
Number of pages23
Publication statusPublished - 1982

Publication series

NameVerslag / RIKILT
No.82.48

    Fingerprint

Keywords

  • determination
  • anabolics
  • growth promoters
  • anabolic steroids
  • urine
  • urine analysis
  • liquid chromatography
  • hptlc
  • faeces
  • electrochemistry

Cite this

van der Struijs, T. B. D., Hooijerink, H., Weseman, J. M., Binnendijk, G. M., van Leeuwen, A. G., Vonk, D. J., & de Ruig, W. G. (1982). The determination of DES and other anabolica in urine and faeces by LC-EC and by HPTLC. (Verslag / RIKILT; No. 82.48). Wageningen: RIKILT.