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Abstract
Flow injection combined with tandem mass spectrometry (MS/MS) was investigated for the rapid detection of highly polar pesticides that are not amenable to multi-residue methods because they do not partition into organic solvents and require dedicated chromatographic conditions. The pesticides included in this study were amitrole, chlormequat, cyromazine, daminozide, diquat, ethephon, fosetyl-Al, glufosinate, glyphosate and its metabolite aminomethylphosphonic acid, maleic hydrazide, mepiquat and paraquat. The composition of the flow-injection solvent was optimized to achieve maximum MS/MS sensitivity. Instrumental limits of detection varied between
Original language | English |
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Pages (from-to) | 6817-6825 |
Journal | Analytical and Bioanalytical Chemistry |
Volume | 406 |
Issue number | 27 |
DOIs | |
Publication status | Published - 2014 |
Keywords
- liquid-chromatography
- aminomethylphosphonic acid
- quantitative-analysis
- sample preparation
- maleic hydrazide
- lc-ms/ms
- glyphosate
- cereals
- vegetables
- dilution
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Dive into the research topics of 'Rapid detection of pesticides not amenable to multi-residue methods by flow injection-tandem mass spectrometry'. Together they form a unique fingerprint.Projects
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Methodeontwikkeling, accreditatiebehoud en surveys milieucontaminanten en gewasbeschermingsmiddelen t.b.v. WOT (WOT-02-001-017, WOT-02-001-046)
Rijk, J. (Project Leader)
1/01/08 → 31/12/25
Project: LVVN project