Full-Scan Accurate Mass Selectivity of Ultra-Preformance Liquid Chromatography Combined with Time-of-Flight and Orbitrap Mass Spectrometry in Hormone and Veterinary Drug Residue Analysis

E. van der Heeft, Y.J.C. Bolck, B. Beumer, A.W.J.M. Nijrolder, A.A.M. Stolker, M.W.F. Nielen

Research output: Contribution to journalArticleAcademicpeer-review

131 Citations (Scopus)

Abstract

The applicability of ultra-performance liquid chromatography (UPLC) combined with full-scan accurate mass time-of-flight (TOF) and Orbitrap mass spectrometry (MS) to the analysis of hormone and veterinary drug residues was evaluated. Extracts from blank bovine hair were fortified with 14 steroid esters. UPLC-Orbitrap MS performed at a resolving power of 60,000 (FWHM) enabled the detection and accurate mass measurement (
Original languageEnglish
Pages (from-to)451-463
Number of pages13
JournalJournal of the American Society for Mass Spectrometry
Volume20
DOIs
Publication statusPublished - 2009

Keywords

  • screening method
  • urine
  • bovine
  • agents

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