Comprehensive Gas Chromatography of High-Boiling Halogenated Compounds

H.J. de Geus, J. de Boer, U.A.T. Brinkman

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    15 Citations (Scopus)

    Abstract

    Comprehensive gas chromatography is an excellent technique for separating complex mixtures. If, however high-boiling compounds such as polychlorinated biphenyls have to be analysed, proper adjustiment of the temperature of the modulator turns out to be very important in maintaining the performance of the system. It is shown that miniaturisation of the column-to-modulator coupling, adequate selection of the modulating conditions and, for halogenated compound mixtures, the use of a micro electron-capture detector, can solve experimental problems previously encountered with high boilers.
    Original languageEnglish
    Pages (from-to)339-344
    JournalChromatographia
    Volume55
    Issue number5/6
    DOIs
    Publication statusPublished - 2002

    Keywords

    • gaschromatography
    • Halogenated compounds

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  • Cite this

    de Geus, H. J., de Boer, J., & Brinkman, U. A. T. (2002). Comprehensive Gas Chromatography of High-Boiling Halogenated Compounds. Chromatographia, 55(5/6), 339-344. https://doi.org/10.1007/BF02491669